aluminium trichloride 5 h; Heating;

aluminium trichloride

hydrogen; palladium on activated charcoal in ethanol T=65°C; 24 h; atmospheric pressure;

1: 99 percent / H2 / Pd/C / ethanol / 24 h / 65 °C / atmospheric pressure 2: acetyl chloride / Heating View Scheme

1.1: 99 percent / H2 / Pd/C / ethanol / 24 h / 65 °C / atmospheric pressure 2.1: acetyl chloride / Heating 3.1: 105.71 g / i-PrMgCl / tetrahydrofuran / 0.58 h / -10 °C 4.1: i-PrMgCl / bis-(2-methoxy-ethyl) ether; tetrahydrofuran / 0.83 h / -5 °C 4.2: 43 percent / bis-(2-methoxy-ethyl) ether; tetrahydrofuran / 20 h / 82 °C View Scheme

View Scheme