甲基-beta-D-呋喃核糖苷合成路线 （共 28 条）
反应条件
1: 98 percent / trimethylsilylazide, stannic chloride / CH2Cl2 / 48 h / Ambient temperature 2: 90 percent / sodium / 12 h / Ambient temperature View Scheme
参考文献
Farmaco, , vol. 47, # 5 p. 525 - 536
反应条件
1: nitrosonium hexafluorophosphate / acetonitrile / 0.25 h / 0 °C 2: 1.) NaHCO3 (aq.), 2.) NaOCH3 / 2.) CH3OH View Scheme
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 38, # 2 p. 157 - 164
反应条件
1: 0.8 g / NaN3 / dimethylformamide / 6 h / 90 °C 2: nitrosonium hexafluorophosphate / acetonitrile / 0.25 h / 0 °C 3: 1.) NaHCO3 (aq.), 2.) NaOCH3 / 2.) CH3OH View Scheme
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 38, # 2 p. 157 - 164
反应条件
1: 2.) pyridine 2: 0.8 g / NaN3 / dimethylformamide / 6 h / 90 °C 3: nitrosonium hexafluorophosphate / acetonitrile / 0.25 h / 0 °C 4: 1.) NaHCO3 (aq.), 2.) NaOCH3 / 2.) CH3OH View Scheme
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 38, # 2 p. 157 - 164
反应条件
1: 92 percent / HgBr2, pyridinium toluene-p-sulphonate / CH2Cl2; methanol / Heating 2: 82 percent / KOH / methanol / 0.5 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 11 p. 2707 - 2716
反应条件
in tetrachloromethane 24 h; Ambient temperature; Yield given;
参考文献
Tetrahedron Letters, , vol. 31, # 43 p. 6193 - 6196
反应条件
hydrogenchloride Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 31, # 31 p. 4437 - 4440
反应条件
1: 86 percent / methanol, sodium / 12 h / Ambient temperature 2: 89 percent / sodium / 1.) reflux, 3 h, 2.) RT, overnight View Scheme
参考文献
Farmaco, , vol. 47, # 5 p. 525 - 536
反应条件
sodium methylate; sodium hydrogencarbonate 2.) CH3OH; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 38, # 2 p. 157 - 164
参考文献
Canadian Journal of Chemistry, , vol. 41, p. 2743,2756
