3-(2,4,6-三甲氧基苯基)丙酸合成路线 (共 4 条)
反应条件
gold(III) chloride; silver trifluoromethanesulfonate in 1,2-dichloro-ethane
T=80°C;
参考文献
Li, Zigang; Shi, Zhangjie; He, Chuan
Journal of Organometallic Chemistry, 2005 , vol. 690, # 23 p. 5049 - 5054
反应条件
1: With sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene in water; tert-butyl alcohol
T=0 - 20°C; Pinnick oxidation; Inert atmosphere;
2: With ammonium chloride in water; tert-butyl alcohol
T=20°C; Inert atmosphere;
参考文献
Maki, Brooks E.; Scheldt, Karl A.
Organic Letters, 2008 , vol. 10, # 19 p. 4331 - 4334
反应条件
sulfuric acid in diethyl ether
参考文献
Donnelly,J.A.; Maloney,D.E.
Tetrahedron, 1979 , vol. 35, p. 2883 - 2888
反应条件
sodium hydroxide; ethanol
参考文献
Nakazawa; Matsuura
Yakugaku Zasshi, 1955 , vol. 75, p. 68,71
Chem.Abstr., 1956 , p. 978