5,6-二氢-2H-1,4-恶嗪-3-胺合成路线 (共 3 条)
反应条件
1: in acetonitrile
T=30 - 35°C; 2 - 2.5 h;
2: With potassium carbonate in acetonitrile
T=70°C; 0.25 - 0.5 h; Product distribution / selectivity;
参考文献
Wyeth
Patent: US2009/18332 A1, 2009 ;
Location in patent: Page/Page column 4; 13-14 ;
US 20090018332 A1
反应条件
T=30 - 70°C; 1 - 1.5 h; Product distribution / selectivity;
参考文献
Wyeth
Patent: US2009/18332 A1, 2009 ;
Location in patent: Page/Page column 14 ;
US 20090018332 A1
反应条件
1: in acetonitrile
T=30 - 35°C; 2 - 2.5 h;
2: With potassium carbonate in acetonitrile
T=70°C; 0.25 - 0.5 h; Product distribution / selectivity;
参考文献
Wyeth
Patent: US2009/18332 A1, 2009 ;
Location in patent: Page/Page column 4; 13-14 ;
US 20090018332 A1