1: 76 percent / AlCl3 / 0.5 h / Heating 2: 75 percent / H2O, conc. HCl, amalgamated zinc / toluene / 28 h / Heating 3: PCl5 4: AlCl3 / benzene / 1.) 5 deg C, 1 h, 2.) room temperature, 3 h 5: Mg / diethyl ether / 16 h / -2 °C View Scheme

trifluorormethanesulfonic acid T=65 - 95°C; 55 h;

water T=25°C;

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