bromine in tetrachloromethane slow addn. of bromine in CCl4 to a soln. of Sb-compd. in CCl4 at -5°C over 30 min in a N2 atmosphere, colour of bromine disappears readily after each addn., but at the end a light brown colour persists; warming to room temp., removal of volatiles in vacuo, monitoring residue by IR;
参考文献
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, , vol. 23, p. 1363 - 1378
Baker et al.
Journal of Organic Chemistry, 1952 , vol. 17, p. 149,153
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Sadler; Warren
Journal of the American Chemical Society, 1956 , vol. 78, p. 1251,1254
