1-(4-氯苯基)乙烷-1,2-二醇合成路线 (共 16 条)
反应条件
β-cyclodextrin; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in water; acetone T=20°C; 12 h;
参考文献
Surendra; Srilakshmi Krishnaveni; Arjun Reddy; Nageswar; Rama Rao
Journal of Organic Chemistry, 2003 , vol. 68, # 5 p. 2058 - 2059
反应条件
di-isopropyl azodicarboxylate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25 - 40°C; Mitsunobu cyclodehydration; 2 h;
参考文献
Weissman; Rossen; Reider
Organic letters, 2001 , vol. 3, # 16 p. 2513 - 2515
反应条件
1: various solvent(s) / 22 h / 25 °C / lipase PS on Celite 577 2: NaOH / methanol / 3 h / 25 °C View Scheme
参考文献
Bosetti, Aldo; Bianchi, Daniele; Cesti, Pietro; Golini, Paolo; Spezia, Sandro
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 18 p. 2395 - 2398
反应条件
dihydrogen peroxide; ethyl acetate; lipase [PSLG6] in water
T=60°C; 0.0833333 h; microwave irradiation;
参考文献
Sarma, Kuladip; Borthakur, Naleen; Goswami, Amrit
Tetrahedron Letters, 2007 , vol. 48, # 38 p. 6776 - 6778
反应条件
sodium tetrahydroborate in ethanol
1 h;
参考文献
Mahajabeen, Pula; Chadha, Anju
Tetrahedron Asymmetry, 2011 , vol. 22, # 24 p. 2156 - 2160
反应条件
iodine; aminopropyl silica gel in water; acetonitrile
T=25°C; 0.75 h;
参考文献
Tamami; Iranpoor; Mahdavi
Synthetic Communications, 2002 , vol. 32, # 8 p. 1251 - 1258
反应条件
1: With water in chloroform
T=40°C;
2: With water; sodium hydroxide in chloroform
T=40°C; 18 h;
参考文献
Jones, Kevin M.; Tomkinson, Nicholas C. O.
Journal of Organic Chemistry, 2012 , vol. 77, # 2 p. 921 - 928
反应条件
Oxonereg;; C16H22Cl2FeN4(2+); sodium hydrogencarbonate in water; acetonitrile
T=20°C; 0.0833333 h;
参考文献
Chow, Toby Wai-Shan; Wong, Ella Lai-Ming; Guo, Zhen; Liu, Yungen; Huang, Jie-Sheng; Che, Chi-Ming
Journal of the American Chemical Society, 2010 , vol. 132, # 38 p. 13229 - 13239
反应条件
oxygen; bismuth mandelate in dimethyl sulfoxide
T=80°C; P=760 Torr; 7 h; Rate constant;
参考文献
Boisselier, Veronique Le; Dunach, Elisabet; Postel, Michele
Journal of Organometallic Chemistry, 1994 , vol. 482, # 1-2 p. 119 - 124
反应条件
dihydrogen peroxide; lipase [PSLG6] in water
Heating;
参考文献
Sarma, Kuladip; Borthakur, Naleen; Goswami, Amrit
Tetrahedron Letters, 2007 , vol. 48, # 38 p. 6776 - 6778