in neat (no solvent) (dry Ar); sealed ampul; heated for 40 h at 100°C; ppt. Et2NH2Br filtered; washed (Et2NH); filtrate heated for 100 h; additional isolatedEt2NH2Br; filtrate distn.; elem. anal.;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 29, # 5 p. 813 - 820
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 5 p. 1106 - 1113
