6-(苯二甲酰亚氨基甲基)吗吩烷啶合成路线 (共 2 条)
反应条件
in N,N-dimethyl-formamide T=80°C; 4 h;
参考文献
Moffett
Journal of Heterocyclic Chemistry, 1980 , vol. 17, # 2 p. 341 - 350
反应条件
1: N-lt;(11H-dibenzlt;b,egt;azepin-6-yl)methylgt;phthalimide With sodium tetrahydroborate in methanol; water; isopropyl alcohol; toluene T=20 - 30°C; 24.5 h; 2: With hydrogenchloride in water; isopropyl alcohol T=20 - 80°C; 1.5 h; 3: (2E)-but-2-enedioic acid With sodium hydroxide Product distribution / selectivity; more than 3 stages;
参考文献
Konica Minolta Chemical Co., Ltd.
Patent: EP1496051 A1, 2005 ;
Location in patent: Page 3 ;