(+/-)-2,2-二溴-1,1-二联萘合成路线 (共 37 条)
参考文献
Journal of the American Chemical Society, , vol. 102, # 27 p. 7932 - 7934
反应条件
lead(IV) acetate; boron trifluoride diethyl etherate in acetonitrile 3 h;
参考文献
Journal of the American Chemical Society, , vol. 102, # 21 p. 6504 - 6512
反应条件
tert.-butylnitrite; copper(I) bromide in acetonitrile T=65°C; 3 h;
参考文献
Tetrahedron Asymmetry, , vol. 24, # 15-16 p. 894 - 902
反应条件
bromine; triphenylphosphine in acetonitrile T=230 - 300°C;
参考文献
Tetrahedron, , vol. 60, # 20 p. 4387 - 4397
反应条件
bromine in acetonitrile microwave irradiation;
参考文献
Synthetic Communications, , vol. 33, # 16 p. 2763 - 2767
反应条件
phosphorus tribromide T=310°C;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 17 p. 1323 - 1325
反应条件
acetonitrile, 60 deg C, 30 min then 260-270 deg C, 1 h then 311-320 deg C, 1 h; Yield given;
参考文献
Tetrahedron, , vol. 40, # 8 p. 1245 - 1253
反应条件
copper(l) iodide; sodium azide; N-methyl-2-(methylamino)ethylamine in dimethyl sulfoxide T=100°C; 48 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 75, # 14 p. 4887 - 4890
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 1 h; Inert atmosphere; 2: With methanol in tetrahydrofuran; hexane T=-78 - 23°C; Inert atmosphere;
参考文献
Wang, Yahui; McGonigal, Paul R.; Herle, Bart; Besora, Maria; Echavarren, Antonio M.
Journal of the American Chemical Society, 2014 , vol. 136, # 2 p. 801 - 809