反应条件
1: [4-chloro-3,6-difluoro-2-(methoxymethoxy)phenyl]trimethylsilane With 2,2,6,6-tetramethyl-piperidine; n-butyllithium in tetrahydrofuran; hexane
T=-75°C; 2 h;
2: carbon dioxide in tetrahydrofuran; hexane
3: With hydrogenchloride
pH=1;
参考文献
Marzi, Elena; Gorecka, Joanna; Schlosser, Manfred
Synthesis, 2004 , # 10 p. 1609 - 1618