反应条件
1: 83 percent / lithium triethylborohydride / dimethylsulfoxide; tetrahydrofuran / 14 h / 35 °C
2: 96 percent / triethylamine; 4-(dimethylamino)pyridine / dimethylformamide / 24 h / 45 °C
3: 60 percent / diethylaminosulfur trifluoride / CH2Cl2 / 0.5 h / 40 °C
4: 69 percent / hydrochloric acid / CH2Cl2; methanol / 1.5 h / 30 °C
5: 67 percent / 2-mercaptoethanol; NaOMe / methanol / 48 h / 50 °C
View Scheme
参考文献
Torii, Takayoshi; Onishi, Tomoyuki; Izawa, Kunisuke; Maruyama, Tokumi; Demizu, Yosuke; Neyts, Johan; De Clercq, Erik
Nucleosides, Nucleotides and Nucleic Acids, 2006 , vol. 25, # 4-6 p. 655 - 665
