4,5-二氯-2-硝基甲苯合成路线 （共 15 条）
反应条件
1: bei der Reduktion
View Scheme
参考文献
Cohen; Dakin
Journal of the Chemical Society, 1902 , vol. 81, p. 1335
Journal of the Chemical Society, 1906 , vol. 89, p. 1454
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane
120 h; Heating / reflux;
参考文献
Active Biotech AB
Patent: US2005/192288 A1, 2005 ;
Location in patent: Page/Page column 6 ;
反应条件
N-bromosuccinmide; dibenzoyl peroxide in benzene
14 h; Heating;
参考文献
Chen, Jiong J.; Drach, John C.; Townsend, Leroy B.
Journal of Organic Chemistry, 2003 , vol. 68, # 11 p. 4170 - 4178
反应条件
1: With N,N-dimethyl-formamide dimethyl acetal
T=140°C; 24 h; RefluxInert atmosphere;
2: With sodium periodate in water; N,N-dimethyl-formamide
T=20°C; 4 h;
参考文献
Ramalingam, Bose Muthu; Saravanan, Velu; Mohanakrishnan, Arasambattu K.
Organic Letters, 2013 , vol. 15, # 14 p. 3726 - 3729
参考文献
Kenner; Tod; Witham
Journal of the Chemical Society, 1925 , vol. 127, p. 2348
