2,2',3,3'-四甲基联苯合成路线 （共 11 条）
反应条件
chloroethylmethylchloride; anhydrous iron chloride in tetrahydrofuran
T=30 - 50°C; 3 h; Product distribution / selectivity;
参考文献
Toray Fine Chemicals Co., Ltd.; Haqyashi, Tamio
Patent: EP2075241 A1, 2009 ;
Location in patent: Page/Page column 7 ;
反应条件
nickel trifluoromethanesulfonate; lithium; magnesium; ethylene dibromide in tetrahydrofuran
T=20°C; RefluxInert atmosphere;
参考文献
Lv, Dan; Zhang, Yan-Yan; Li, Jing-Hua
Journal of Chemical Research, 2009 , # 6 p. 397 - 399
反应条件
iron(III) trifluoromethanesulfonate; magnesium in tetrahydrofuran
T=20°C; 4 h;
参考文献
Zhang, Yan-Yan; Lin, Jing-Du; Xu, Xiao-Liang; Li, Jing-Hua
Synthetic Communications, 2010 , vol. 40, # 17 p. 2556 - 2563
反应条件
triphenylphosphine; niobium bromide in tetrahydrofuran
Heating;
参考文献
House; Holt; VanDerveer
Journal of Organic Chemistry, 1993 , vol. 58, # 26 p. 7516 - 7523
反应条件
Nafion-H; toluene
12 h; Heating;
参考文献
Olah, George A.; Prakash, G. K. Surya; Iyer, Pradeep S.; Tashiro, Masashi; Yamato, Takehiko
Journal of Organic Chemistry, 1987 , vol. 52, # 9 p. 1881 - 1884
反应条件
Nafion-H
12 h; Heating;
参考文献
Olah, George A.; Prakash, G. K. Surya; Iyer, Pradeep S.; Tashiro, Masashi; Yamato, Takehiko
Journal of Organic Chemistry, 1987 , vol. 52, # 9 p. 1881 - 1884
反应条件
aluminium trichloride; nitromethane in benzene
参考文献
Tashiro,M.; Yamato,T.
Journal of Organic Chemistry, 1979 , vol. 44, p. 3037 - 3041
参考文献
Newman,M.S.; Wiseman,E.H.
Journal of Organic Chemistry, 1961 , vol. 26, p. 3208 - 3211
反应条件
1: (iodination)
2: Cu / 300 °C
3: AlCl3, MeNO2 / benzene
View Scheme
参考文献
Tashiro,M.; Yamato,T.
Journal of Organic Chemistry, 1979 , vol. 44, p. 3037 - 3041
反应条件
1: Cu / 300 °C
2: AlCl3, MeNO2 / benzene
View Scheme
参考文献
Tashiro,M.; Yamato,T.
Journal of Organic Chemistry, 1979 , vol. 44, p. 3037 - 3041
