4,5-乙撑二硫代-1,3-二硫酚-2-酮合成路线 (共 45 条)
反应条件
phosphorous acid trimethyl ester
T=65°C; 5 h; Title compound not separated from byproducts;
参考文献
Mori, Takehiko; Inokuchi, Hiroo; Kini, Aravinda M.; Williams, Jack M.
Chemistry Letters, 1990 , # 8 p. 1279 - 1282
反应条件
triethyl phosphite
1 h; Heating;
参考文献
Abashev, G. G.; Russkikh, V. S.; Shklyaeva, E. V.; Vladykin, V. I.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 11 p. 1533 - 1537
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 11 p. 1705 - 1710
反应条件
phosphorous acid trimethyl ester
Heating;
参考文献
Noh, Dong-Youn; Han, Sung-Won; Lee, Ha-Jin; Jung, Dongwoon; Kang, Woun
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2002 , vol. 380, p. 123 - 128
反应条件
1: 30 percent / trimethyl phosphite / benzene / 4 h / Heating
2: 36 percent / lithium bromide / hexamethylphosphoric acid triamide / 0.25 h / 150 °C
View Scheme
参考文献
Papavassiliou, G.C.; Zambounis, J.S.; Mousdis, G.A.; Gionis, V.; Yiannopoulos, S.Y.
Molecular Crystals and Liquid Crystals (1969-1991), 1988 , vol. 156, p. 269 - 276
参考文献
Kato, Reizo; Kobayashi, Hayao; Kobayashi, Akiko
Chemistry Letters, 1989 , p. 781 - 784