disodium hydrogenphosphate; sodium amalgam in tetrahydrofuran; methanol
14 h;
参考文献
Michael, Joseph P.; De Koning, Charles R.; Malefetse, Tshepo J.; Yillah, Ibrahim
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 23 p. 3510 - 3517
1: tetrahydrofuran / 17 h / 0 °C
2: Et3N / CH2Cl2 / 72 h / 20 °C
3: KOH / ethanol / 0.5 h / Heating
4: 183 mg / Ac2O; K2CO3 / acetonitrile / 23 h
5: 77 percent / sodium amalgam; Na2HPO4 / tetrahydrofuran; methanol / 14 h
View Scheme
参考文献
Michael, Joseph P.; De Koning, Charles R.; Malefetse, Tshepo J.; Yillah, Ibrahim
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 23 p. 3510 - 3517
1: phosphorus pentasulfide
2: tetrahydrofuran / 17 h / 0 °C
3: Et3N / CH2Cl2 / 72 h / 20 °C
4: KOH / ethanol / 0.5 h / Heating
5: 183 mg / Ac2O; K2CO3 / acetonitrile / 23 h
6: 77 percent / sodium amalgam; Na2HPO4 / tetrahydrofuran; methanol / 14 h
View Scheme
参考文献
Michael, Joseph P.; De Koning, Charles R.; Malefetse, Tshepo J.; Yillah, Ibrahim
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 23 p. 3510 - 3517
Michael, Joseph P.; De Koning, Charles R.; Malefetse, Tshepo J.; Yillah, Ibrahim
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 23 p. 3510 - 3517
Goti, Andrea; Brandi, Alberto; Danza, Giovanna; Guarna, Antonio; Donati, Donato; Sarlo, Francesco De
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 1253 - 1258
