Kozhushko, B. N.; Gumenyuk, A. V.; Mikhailyuchenko, N. K.; Shokol, V. A.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 3 p. 541 - 549,430 - 437
byproducts: POCl3; portionwise addn. of PCl5 at 75-100°C (14 h); distn. of OPCl3 at 760 Torr; heating to 140°C; further addn. of PCl5;
参考文献
Frank, A. W.
Journal of Organic Chemistry, 1966 , vol. 31, p. 1521 - 1524
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Gmelin Handbook: F: PerFHalOrg.3, 1.8, page 51 - 70
O2; CuCl2; HCl in neat (no solvent) Kinetics; byproducts: H2O; a satd. alcoholic soln. of HCl was loaded together with CuCl2 into the reactor and purged with an Ar-O2 mixture; then Cu3P was added and the mixt. reacted at 323 K;;
参考文献
Kinetics and Catalysis, , vol. 33, p. 243 - 251
Kinetika i Kataliz, , vol. 33, p. 304 - 313
