in ethylene glycol dimethyl ether
T=25°C; Rate constantKinetics;
参考文献
Solov'yanov, A. A.; Karpyuk, A. D.; Sizov, A. Yu.; Beletskaya, I. P.; Reutov, O. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 8 p. 1461 - 1466
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 8 p. 1605 - 1611
water in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide
soln. of Ph2GeK2 in HMPA/THF added to EtCl, stirred at room temp. for 30 min, cooled with water bath, hydrolyzed; extd. with ether, org. layer dried over anhyd. Na2SO4, isolated by preparative GLC and TLC;
参考文献
Mochida, Kunio; Matsushige, Naoki; Hamashima, Mari
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 5 p. 1443 - 1447
Galiakhmetov, R. N.; Valitov, R. B.; Kurochkin, A. K.; Margulis, M. A.
Russian Journal of Physical Chemistry, 1986 , vol. 60, # 4 p. 614 - 615
Zhurnal Fizicheskoi Khimii, 1986 , vol. 60, p. 1024 - 1025
