Na in diethyl ether introduction of vinylchloride into a ether soln. of (CH3)3SiCl in presence of dispersed Na and ethylacetate as catalyst;;
参考文献
Kanazashi, M.
Bulletin of the Chemical Society of Japan, 1953 , vol. 26, p. 493 - 496
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Gmelin Handbook: Si: MVol.C, 15, page 44 - 48
sodium sulfide; potassium hydroxide in dimethyl sulfoxide T=90 - 100°C; 6 h; Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Trofimov, B. A.; Amosova, S. V.; Nosyreva, V. V.; Voronkov, M. G.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 11 p. 2123 - 2127
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 11 p. 2324 - 2328
sodium sulfide; potassium hydroxide in dimethyl sulfoxide T=90 - 100°C; 4 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Trofimov, B. A.; Amosova, S. V.; Nosyreva, V. V.; Voronkov, M. G.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 11 p. 2123 - 2127
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 11 p. 2324 - 2328
sodium sulfide; potassium hydroxide in dimethyl sulfoxide T=90 - 100°C; 4 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Trofimov, B. A.; Amosova, S. V.; Nosyreva, V. V.; Voronkov, M. G.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 11 p. 2123 - 2127
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 11 p. 2324 - 2328
