potassium hydroxide in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=110°C; 3 h;
参考文献
Aliev, I. A.; Mikhaleva, A. I.; Bairamova, S. Kh.; Akhmedov, E. I.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, p. 433 - 435
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 3 p. 489 - 492
in benzene under Ar atm. using Schlenk techniques; a flask was charged with Ni complex in benzene; vinyl chloride was condensed into the tube at -78°C under vac.; soln. stirred for 4 ds at 50°C; cooled to room temp.; volatiles removed (vac.); filtered; filtrate was left to stand at 25°C for 24 h; red brown crystals pptd. and sepd. by filtration; filtrate heated to 50°C for 4 ds; filtered; condensed under vac.; cooled to -36°C; dark red crystals;
参考文献
Journal of the American Chemical Society, , vol. 125, # 14 p. 4350 - 4361
