1: in tetrahydrofuran; methanol T=20°C; 24 h; 2: With sodium tetrahydroborate in tetrahydrofuran; methanol T=20°C; 3 h; 3: With hydrogenchloride; sodium hydrogencarbonate more than 3 stages;
1: in tetrahydrofuran 2: With hydrogenchloride in diethyl ether; water
参考文献
Power, John D.; McDermott, Sean D.; Talbot, Brian; O'Brien, John E.; Kavanagh, Pierce
Rapid Communications in Mass Spectrometry, 2012 , vol. 26, # 22 p. 2601 - 2611
