反应条件
in acetonitrile Electrochem. Process; the anode compartment of the electrochemical cell was charged with (NBu(n)4)(B9H12) (1.0 mmol) dissolved in MeCN; the cathode compartment contained a soln. of (NBu(n)4)(BF4) in MeCN;; the solvent was removed under reduced pressure and the solid examd. by t.l.c. on silica (CH2Cl2 eluant);;
参考文献
Jacobsen, Grant B.; Meina, Dominic G.; Morris, John H.; Thomson, Colin; Andrews, Steven J.; et al.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1985 , p. 1645 - 1654