ammonia in acetonitrile neopentylSnMe3 in CH3CN added to Fe(phen)3(PF6)3 in CH3CN at 22°C under Ar and soln. stirred for 2 h, drop water added and Fe(II) complex filtered, filtrate dried with MgSO4 and treated anhyd. NH3 and Sn product filtered;
参考文献
Journal of the American Chemical Society, , vol. 104, # 5 p. 1319 - 1330
NOBF4 in water 15-30 min; Further byproducts given. Yields of byproduct given;
参考文献
Blankespoor, Ronald L.; Doyle, Michael P.; Smith, Daniel J.; Dyke, David A. Van; Waldyke, Michael J.
Journal of Organic Chemistry, 1983 , vol. 48, # 8 p. 1176 - 1179