in acetonitrile at 20-25°C (according to Bull. Chem. Soc. Jpn 1971, 44, 2555-2556);
参考文献
Angewandte Chemie - International Edition, , vol. 43, # 23 p. 3056 - 3058
→
反应条件
ammonia in acetonitrile t-BuSnMe3 in CH3CN added to Fe(phen)3(ClO4)3 in CH3CN at 22°C under Ar and soln. stirred for 2 h, drop water added, Fe(II) complex filtered, filtrate dried with MgSO4 and treated with anhyd. aq. NH3, Sn product treated with HCl and sublimed;
参考文献
Journal of the American Chemical Society, , vol. 104, # 5 p. 1319 - 1330
thianthrenium perchlorate Ambient temperature; Further byproducts given;
参考文献
Bae, Dong Hak; Engel, Paul S.; Hoque, A. K. M. Mansurul; Keys, Dalen E.; Lee, Wang-Keun; et al.
Journal of the American Chemical Society, 1985 , vol. 107, # 8 p. 2561 - 2562
thianthrene cation radical perchlorate Ambient temperature; Further byproducts given;
参考文献
Shine, Henry J.; Bae, Dong Hak; Hoque, A. K. M. Mansurul; Kajstura, Alojzy; Lee, Wang Keun; et al.
Phosphorus and Sulfur and the Related Elements, 1985 , vol. 23, p. 111 - 142
thianthrenium perchlorate Ambient temperatureeffect of molar ratio; MechanismProduct distribution;
参考文献
Bae, Dong Hak; Engel, Paul S.; Hoque, A. K. M. Mansurul; Keys, Dalen E.; Lee, Wang-Keun; et al.
Journal of the American Chemical Society, 1985 , vol. 107, # 8 p. 2561 - 2562
T=50°C; 960 h; other temperature;various quaternary or alkali salts added, with/without water. Other object of study: energy data (ΔH<*>, ΔS<*>, ΔG<*>); influence of the (in)organic salt added; MechanismProduct distributionKinetics;
参考文献
Ponomareva, E. A.; Tarasenko, P. V.; Yurchenko, A. G.; Dvorko, G. F.
Journal of Organic Chemistry USSR (English Translation), 1983 , p. 2191 - 2203
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 12 p. 2503 - 2516
