Kim, Sun Min; Jin, Ming Yu; Kim, Mi Jin; Cui, Yan; Kim, Young Sug; Zhang, Liqiu; Song, Choong Eui; Ryu, Do Hyun; Yang, Jung Woon
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 7 p. 2069 - 2071
1: 2-bromo-pyridine With n-butyllithium; diisopropylamine in tetrahydrofuran; hexane
T=-78°C; 1 h;
2: acetaldehyde in tetrahydrofuran; hexane
T=-78°C; 1 h;
3: With ammonium chloride in tetrahydrofuran; hexane; water
Saturated solution;
参考文献
MERCH SHARP and DOHME LIMITED
Patent: WO2006/59149 A1, 2006 ;
Location in patent: Page/Page column 22-23 ;
WO 2006/059149 A1
