反应条件
sodium hydroxide in ethanol soln. ethanethiol and NaOH in EtOH was added dropwise to soln. (2-bromomethylphenyl)boronic acid pinacol ester in EtOH and stirreed for 30 min at room temp.; solvent was evapd., residue was purified by column chromy. on silica (hexane:EtOAc 20:1);
参考文献
Cody, John; Dennisson, Jeanette; Gilmore, Joshua; VanDerveer, Donald G.; Henary, Maged M.; Gabrielli, Alan; Sherrill, C. David; Zhang, Yiyun; Pan, Chia-Pin; Burda, Clemens; Fahrni, Christoph J.
Inorganic Chemistry, 2003 , vol. 42, # 16 p. 4918 - 4929
