反应条件
Zn; CuSO4; acetic acid in tetrahydrofuran CH2I2 is added under N2 to Zn-Cu couple (prepd. from Zn and CuSO4, in acetaic acid heating on steam bath for 2 min) in THF, stirring for 4 h, cooling to 0°C, filtn. (N2, glass wool), then Sn(CH3)3Cl is added, stirring overnight.; Adding aq. HCl and benzene, collecting the organic layer, washing with HCl and drying over Na2SO4, evapn., distn.;
参考文献
Cox, Philip J.; Doidge-Harrison, Solange M. S. V.; Howie, R. Alan; Nowell, Ian W.; Taylor, Oonah J.; Wardell, James L.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry, 1989 , p. 2017 - 2022
