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1: diiodomethane With diethylzinc; 2,4,6-Trichlorophenol in hexanes; dichloromethane T=-40°C; 0.5 h; 2: 3-Bromostyrene in hexanes; dichloromethane T=20°C; 3: With potassium permanganate; water in tetrahydrofuran T=0 - 20°C; 1 h;
参考文献
ASTRA ZENECA AB; NPS PHARMACEUTICALS, INC.
Patent: WO2004/14881 A2, 2004 ;
Location in patent: Page 136-137 ;
WO 2004/014881 A2
