1: diiodomethane With diethylzinc in dichloromethane
T=0°C; 0.25 h;
2: 3,3-dimethylallyl alcohol in dichloromethane
T=-20°C; 0.25 h;
3: With titanium tetrachloride in dichloromethane
T=-20°C; 2 h; Further stages.;
参考文献
Charette; Molinaro; Brochu
Journal of the American Chemical Society, 2001 , vol. 123, # 49 p. 12160 - 12167