in toluene
(Ar); using Schlenk techniques; addn. of 1 equiv. of dimethyl sulfide tostirred soln. of Ge(OMes)2(tmeda) in toluene at room temp.; stirring fo r 16 h; removal of solvents in vac.; recrystn. in Et2O;
参考文献
Bonnefille, Eric; Mazieres, Stephane; Hawi, Nancy El; Gornitzka, Heinz; Couret, Claude
Journal of Organometallic Chemistry, 2006 , vol. 691, p. 5619 - 5625
Doren, J. M. Van; Barlow, S. E.; DePuy, C. H.; Bierbaum, V. M.; Dotan, I.; Ferguson, E. E.
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