aluminium; aluminium trichloride in neat (no solvent) in presence of activated Al-powder, H2-pressure 2000 psi, 180°C, 1h;; separation by distn. in vac.;;
参考文献
Ashby, E. C.; Foster, W. E.
Journal of the American Chemical Society, 1962 , vol. 84, p. 3407 - 3408
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Gmelin Handbook: B: B-Verb.14, 3.8, page 77 - 81
lithium borohydride in diethyl ether T=-78 - 20°C;
参考文献
Aldridge, Simon; Downs, Anthony J.; Tang, Christina Y.; Parsons, Simon; Clarke, Michael C.; et al.
Journal of the American Chemical Society, 2009 , vol. 131, p. 2231 - 2243
in diethyl ether byproducts: H2; stirring at room temp. until end of H2-evolution, boiling for 1h, filtration, evapn.;;
参考文献
Schaeffer, G. W.; Anderson, E. B.
Journal of the American Chemical Society, 1949 , vol. 71, p. 2143 - 2145
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Gmelin Handbook: B: B-Verb.14, 3.8, page 77 - 81
Bissot, T. C.; Campbell, D. H.; Parry, R. W.
Journal of the American Chemical Society, 1958 , vol. 80, p. 1868 - 1874
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Gmelin Handbook: B: B-Verb.14, 3.8, page 77 - 81
Bissot, T. C.; Campbell, D. H.; Parry, R. W.
Journal of the American Chemical Society, 1958 , vol. 80, p. 1868 - 1874
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Gmelin Handbook: B: B-Verb.14, 3.4, page 51 - 53
sodium-potassium alloy; sodium in ethylene glycol dimethyl ether reduction with Na/K-alloy (25:75 wt.-percent); 2.5-3h, 0°C;;
参考文献
Gragg, B. R.; Ryschkewitsch, G. E.
Inorganic Chemistry, 1976 , vol. 15, p. 1209 - 1212
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Gmelin Handbook: B: B-Verb.14, 3.8, page 77 - 81
