in mineral oil B(OCH3)3 condensed onto Al(CH3)3 soln. with -196°C trap, opened to closed vol., warmed slowly to room temp. with stirring, repeated twice; pumped into -196°C trap, passed through -132°C into -196°C trap;
参考文献
Shinomoto, Ron; Gamp, Eduard; Edelstein, Norman M.; Templeton, David H.; Zalkin, Allan
Inorganic Chemistry, 1983 , vol. 22, p. 2351 - 2355
[(R)-1,1'-binaphthyl-2,2'-diyldioxy]{bis[(S)-(1-phenylethyl)]amino}phosphine; bis(acetylacetonate)nickel(II) in tetrahydrofuran; hexane T=-20°C; 6 h; Title compound not separated from byproducts;
参考文献
Biswas, Kallolmay; Prieto, Oscar; Goldsmith, Paul J.; Woodward, Simon
Angewandte Chemie - International Edition, 2005 , vol. 44, # 15 p. 2232 - 2234
