1: styrene; trimethylaluminum With methylaluminoxane; (-)-(NMI)2ZrCl2 in dichloromethane; water T=23°C; 2: With oxygen in dichloromethane; water T=0 - 23°C; 3: vinyl acetate With Porcine Pancreas Lipase in tetrahydrofuran T=23°C; 7 h; Further stages.;
1: trimethylaluminum With 1,4-diaza-bicyclo[2.2.2]octane in toluene T=0°C; 2: 4-bromo-benzaldehyde With [(R)-1,1'-binaphthyl-2,2'-diyldioxy]{bis[(S)-(1-phenylethyl)]amino}phosphine; bis(acetylacetonate)nickel(II) in tetrahydrofuran T=5°C; 1 h; Title compound not separated from byproducts;
参考文献
Mata, Yvette; Dieguez, Montserrat; Pamies, Oscar; Woodward, Simon
Journal of Organic Chemistry, 2006 , vol. 71, # 21 p. 8159 - 8165
