sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in ethanol; dichloromethane T=30°C; 0.416667 h; ultrasound cleaner; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
potassium hydroxide in tribromo methane; water an aq. KOH soln. was added to react. mixt. at 25 °C, stirred 2 h; washed (H2O), extd. (Et2O), org. layer was dried (anhyd. MgSO4), filtered, solvent was removed by rotary evapn., recrystd. (Et2O/petroleum ether); elem. anal.;
参考文献
Saxena, Arvind K.; Bisaria, Chandra S.; Pande, Lalit M.
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1986 , vol. 16, p. 667 - 674
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in ethanol; dichloromethane T=30°C; 0.416667 h; ultrasound cleaner; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride 1) 2 to 4 deg C, 0.5 h 2) room temperature;
参考文献
Slobodin, Ya. M.; Ashkinazi, L. A.; Klimchuk, G. N.
Journal of Organic Chemistry USSR (English Translation), 1984 , p. 910 - 912
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 5 p. 1001 - 1002
Vitnik, Vesna D.; Milenkovi, Marina T.; Dilber, Sanda P.; Vitnik, Zeljko J.; Juranic, Ivan O.
Journal of the Serbian Chemical Society, 2012 , vol. 77, # 6 p. 741 - 750
