in dimethyl sulfoxide T=30°C; 2.5 h; without crown ethers or in presence of benzo-15-crown-5 or benzo-18-crown-6; other solvent; MechanismProduct distributionRate constant;
参考文献
Whitney, Richard R.; Jaeger, David A.
Tetrahedron, 1980 , vol. 36, p. 769 - 774
in dimethyl sulfoxide T=30°C; 2.5 h; without crown ethers or in presence of benzo-15-crown-5 or benzo-18-crown-6; other solvent; MechanismProduct distributionRate constant;
参考文献
Whitney, Richard R.; Jaeger, David A.
Tetrahedron, 1980 , vol. 36, p. 769 - 774
1: ethyl acetoacetate With potassium tert-butylate in tetrahydrofuran T=0°C; 0.5 h; 2: 2-iodo-propane in tetrahydrofuran T=70°C; 12 h; Further stages.;
参考文献
Beddow, James E.; Davies, Stephen G.; Ling, Kenneth B.; Roberts, Paul M.; Russell, Angela J.; Smith, Andrew D.; Thomson, James E.
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 17 p. 2812 - 2825