反应条件
s-BuLi in tetrahydrofuran; diethyl ether; hexane at -110°C, CF2CH2 + s-BuLi in hexane, THF-Et2O (4:1), stirring (20 min), then ZnCl2 added to the mixt., stirring (-100°C, 30 min); (19)F NMR;
参考文献
Fujita, Takeshi; Ichitsuka, Tomohiro; Fuchibe, Kohei; Ichikawa, Junji
Chemistry Letters, 2011 , vol. 40, # 9 p. 986 - 988
