H2 in perdeuterocyclohexane byproducts: CH3F; under N2; in a resealable NMR tube Zr complex was dissolved in cyclohexane-d12, the tube was freeze-pump-thaw degassed 3 times, CHFCl2 was condensed at -196°C , H2 was added, upon thawing a ppt. formed; not isolated, monitored by NMR;
参考文献
Journal of the American Chemical Society, , vol. 123, # 44 p. 10973 - 10979