ethyleneglykol in 1,2,3,4-tetrahydro-naphthalene 100°C, 15 h;
参考文献
Burg, A. B.; Peterson, L. K.
Inorganic Chemistry, 1966 , vol. 5, p. 943 - 944
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Gmelin Handbook: F: PerFHalOrg.3, 1.1.1, page 1 - 8
H2O; H2O2 in water byproducts: iodine; 30 min shaking with H2O at 20°C excluding air; dropwise addn. of H2O2; filtration; washing (H2O); 5-6 d freeze-drying; sublimation;
参考文献
Gmelin Handbook: F: PerFHalOrg.3, 1.6, page 40 - 51
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Bennett, F. W.; Emeleus, H. J.; Haszeldine, R. N.
Journal of the Chemical Society, 1954 , p. 3598 - 3603