反应条件
(CH3CH2)3N*3HF in N,N-dimethyl-formamide
byproducts: (CH3)3COH, KCl, KF; (Ar); stirring mixt. of 1 equiv. of copper chloride, 1.5-3 equiv. of potassium tert-butoxide, DMF and fluorobenzene as internal standart for 30 min at room temp., addn. of fluoroform, keeping for 5 min, addn. of triethylammonium deriv. in DMF; NMR monitoring;
参考文献
Zanardi, Alessandro; Novikov, Maxim A.; Martin, Eddy; Benet-Buchholz, Jordi; Grushin, Vladimir V.
Journal of the American Chemical Society, 2011 , vol. 133, # 51 p. 20901 - 20913
