反应条件
1: triiodomethane With sodium hexamethyldisilazane in tetrahydrofuran; diethyl ether
T=-78 - -20°C; 1 h; Inert atmosphere;
2: benzyl bromide in tetrahydrofuran; diethyl ether
T=-20°C; 5 h; Inert atmosphere;
3: With potassium tert-butylate in tetrahydrofuran; diethyl ether
T=-20 - 20°C; 12 h; Inert atmosphere;
参考文献
Pelletier, Guillaume; Lie, Sharon; Mousseau, James J.; Charette, Andre B.
Organic Letters, 2012 , vol. 14, # 21 p. 5464 - 5467,4
Title/Abstract Full Text Show Details
Pelletier, Guillaume; Lie, Sharon; Mousseau, James J.; Charette, Andre B.
Organic Letters, 2012 , vol. 14, # 21 p. 5464 - 5467
