反应条件
in diethyl ether; toluene byproducts: NaCl; AlCl3 in ether was added to suspn. NaAlH4 in toluene-ether in 30 min andstired for 4 h, soln. was filtered and cooled to 0°C, Me3N was a dded; solvent was removed;
参考文献
Filippov, Oleg A.; Tsupreva, Victoria N.; Golubinskaya, Lyudmila M.; Krylova, Antonina I.; Bregadze, Vladimir I.; Lledos, Agusti; Epstein, Lina M.; Shubina, Elena S.
Inorganic Chemistry, 2009 , vol. 48, # 8 p. 3667 - 3678
