in benzene under inert gas; 6.06 mmol Me3N in benzene added to 6.04 mmol of the Al compound in benzene; stirring at room temp.; solvent removed in vac.; residue washed with n-pentane and dried in vac.; elem. anal.;
参考文献
Hoffmann, G. G.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1988 , vol. 558, p. 160 - 170
aluminium; aluminium trichloride in neat (no solvent) in presence of activated Al-powder, H2-pressure 2000 psi, 180°C, 1h;; separation by distn. in vac.;;
参考文献
Ashby, E. C.; Foster, W. E.
Journal of the American Chemical Society, 1962 , vol. 84, p. 3407 - 3408
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Gmelin Handbook: B: B-Verb.14, 3.8, page 77 - 81
Bissot, T. C.; Campbell, D. H.; Parry, R. W.
Journal of the American Chemical Society, 1958 , vol. 80, p. 1868 - 1874
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Gmelin Handbook: B: B-Verb.14, 3.8, page 77 - 81
Bissot, T. C.; Campbell, D. H.; Parry, R. W.
Journal of the American Chemical Society, 1958 , vol. 80, p. 1868 - 1874
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Gmelin Handbook: B: B-Verb.14, 3.4, page 51 - 53
