potassium hydroxide in methanol; ethanol
T=-8°C; 0.333333 h;
参考文献
Hall, Robin J.; Shannon, Patrick V. R.; Oliveira-Campos, Ana M.-F.; Queiroz, Maria-Joao R. P.
Journal of Chemical Research, Miniprint, 1992 , # 1 p. 114 - 156
1: nitromethane With sodium hydroxide in methanol
T=0°C; 0.333333 h; Inert atmosphere;
2: 3-chloro-1-phenyl-propan-1-one in methanol
T=0 - 20°C; 5.5 h; Inert atmosphere;
参考文献
O'Connell, Kieron M. G.; Diaz-Gavilan, Monica; Galloway, Warren R. J. D.; Spring, David R.
Beilstein Journal of Organic Chemistry, 2012 , vol. 8, p. 850 - 860
Sonn
Chemische Berichte, 1935 , vol. 68, p. 148,150
Full Text Show Details
Reichert; Posemann
Archiv der Pharmazie (Weinheim, Germany), 1937 , vol. 275, p. 67,78
1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane
T=-65 - 0°C; Michael addition; 0.333333 h;
参考文献
Danilenko, Vitaly M.; Tishkov, Alexander A.; Ioffe, Sema L.; Lyapkalo, Ilya M.; Strelenko, Yury A.; Tartakovsky, Vladimir A.
Synthesis, 2002 , # 5 p. 635 - 647
Buckley et al.
Journal of the Chemical Society, 1947 , p. 1507
Full Text Show Details
Bruson; Riener
Journal of the American Chemical Society, 1943 , vol. 65, p. 26
Full Text Show Details
I.G.Farbenind
Patent: DE728531 , 1940 ;
DRP/DRBP Org.Chem.