in neat (no solvent)
Irradiation (UV/VIS); yield given;;
参考文献
Odum, R. A.; Wolfgang, R.
Journal of the American Chemical Society, 1963 , vol. 85, p. 1050 - 1056
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Gmelin Handbook: C: MVol.D2, 4.2.3.5.6, page 313 - 313
1: n-octanethiol With sodium salt of phosphorous acid in N,N-dimethyl-formamide
0.25 h;
2: monobromotrifluoromethane With hydroxymethanesulfinic acid sodium salt in N,N-dimethyl-formamide
T=20°C; P=3375.27 Torr; 8 h; Title compound not separated from byproducts;
参考文献
Magnier, Emmanuel; Wakselman, Claude
Synthesis, 2003 , # 4 p. 565 - 569