in neat (no solvent) prepared by condensing diborane in small portions to the amine until anexcess of diborane is present as indicated by the vapour pressure; detected by (13)C-NMR;
参考文献
Paz-Sandoval, M. A.; Camacho, C.; Contreras, R.; Wrackmeyer, B.
Spectrochimica Acta, Part A: Molecular and Biomolecular Spectroscopy, 1987 , vol. 43, # 11 p. 1331 - 1336
THE FLORIDA INTERNATIONAL UNIVERSITY BOARD OF TRUSTEES; BECKER, David A.; TAMRAKAR, Relina
Patent: WO2013/67084 A1, 2013 ;
Location in patent: Page/Page column 38 ;