in pentane
dropwise addn. of amine in pentane to borane in pentane at -0°C, stirred for 2 h at room temp.; filtered, distn. (44°C/8 Torr); elem. anal.;
参考文献
Kuepper, Stefan; Paetzold, Peter; Boese, Roland
Chemische Berichte, 1993 , vol. 126, # 8 p. 1787 - 1790
Coyle, Jason P.; Kurek, Agnieszka; Pallister, Peter J.; Sirianni, Eric R.; Yap, Glenn P. A.; Barry, Sean T.
Chemical Communications, 2012 , vol. 48, # 84 p. 10440 - 10442
Marchenko, A. P.; Shaposhnikov, S. I.; Koidan, G. N.; Kharchenko, A. V.; Pinchuk, A. M.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 10 p. 2230 - 2237,1985 - 1992
in petroleum ether
excess of t-butylamine, violent react.;
参考文献
Lappert, M. F.; Majumdar, M. K.
Advances in Chemistry Series, 1964 , vol. 42, p. 208 - 219
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Gmelin Handbook: B: B-Verb.4, 3.3, page 51 - 64
Aubrey,D.W. et al.
Journal of the Chemical Society, 1962 , p. 1786 - 1789
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Gmelin Handbook: B: B-Verb.4, 3.3, page 51 - 64