反应条件
n-butyl lithium in diethyl ether; hexane
N2 atmosphere; metallation of amine with BuLi in hexane (-15°C, 30-60 min), refluxing (2 h), addn. of soln. of Sn-compd. in Et2O (-60°C, 40-60 min), refluxing (2 h); centrifugation (15 min, 1300 rpm), washing (hexane), removal of volatiles from solns. (12 Torr), distn.; elem. anal.;
参考文献
Diemer, Stefan; Noeth, Heinrich; Polborn, Kurt; Storch, Wolfgang
Chemische Berichte, 1992 , vol. 125, # 2 p. 389 - 400
