H2 in neat (no solvent) formation on passing CFCl3 and H2 (molar ratio 1:2) through a glass tube heated to red heat or inflammation of the mixture at the outlet of a capillary; luminescense is observed;;
参考文献
Zeitschrift fuer Anorganische und Allgemeine Chemie, , vol. 201, p. 245 - 258
in not given addn. of HF at -78°C; heating on ambiente temp.;; removing of solvent and HF at 30 - 35°C;;
参考文献
Cavell, R. G.; Clark, H. C.
Journal of the Chemical Society, 1962 , p. 2692 - 2698
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Gmelin Handbook: V: MVol.B1, 66, page 184 - 187