in neat (no solvent) formation on heating to 400 and 500°C with Si in a closed tube; further products;;
参考文献
Barthes, D.; Chaigneau, M.; Malangeau, P.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1968 , vol. 266, p. 1780 - 1783
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Gmelin Handbook: C: MVol.D2, 4.3.2.5.6, page 371 - 372
in neat (no solvent) using a fixed-bed flow reactor system at atmospheric pressure; placing of of V2O3 in quartz reactor; heating at 723 K under 1percent CCl2F2/He atmosphere with total flow rate of 30 ml/min for 5 h; monitoring by XRD and GC-TCD;
参考文献
Tamai, Tsukasa; Inazu, Koji; Aika, Ken-Ichi
Bulletin of the Chemical Society of Japan, 2005 , vol. 78, # 8 p. 1565 - 1574
in neat (no solvent) Electric Arc; decomposition in an electric arc between graphite electrodes (25 V, 18 A, 0.04-0.1 at, 2500-4000°C); reaction also in a graphite furnace at 1500°C;; turnover given;;
in neat (no solvent) atomic calcium was generated by free laser ablation of a rotating Ca sample (1064 nm), 0.7 Torr in scattering cell, 1E-5 Torr in the main chamber; detected by chemiluminescence spectroscopy;
参考文献
Pino; Rinaldi; Ferrero
Chemical Physics Letters, 2001 , vol. 349, # 5-6 p. 463 - 470
