反应条件
water; water-d2 in benzene addn. of a benzene soln. of Li-compd. to a suspension of anhyd. ErCl3 in benzene, stirring at 20 (47-94 h) or 50°C (4.5 h), benzene is completely distd. off in vac., addn. of fresh benzene to solid residue and hydrolysis by H2O or D2O; hydrolysis by H2O: detn. of (CH3)4Si and other Si-org. products by chromy.; hydrolysis by D2O: detn. of undeuterated and deuterated (CH3)4Si bymass spectrometry;
参考文献
Doklady Physical Chemistry (Translation of the physical chemistry section of Doklady Akademii Nauk), , vol. 289 - 291, p. 1023 - 1024
Doklady Akademii Nauk SSSR, , vol. 291, p. 393 - 395
